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Fabrication of bimetallic Cu–Zn adsorbents with high dispersion by using confined space for gas adsorptive

《化学科学与工程前沿（英文）》   页码 1623-1631 doi: 10.1007/s11705-022-2202-y

摘要： The number of active components and their dispersion degree are two key factors affecting the performance of adsorbents. Here, we report a simple but efficient strategy for dispersing active components by using a confined space, which is formed by mesoporous silica walls and templates in the as-prepared SBA-15 (AS). Such a confined space does not exist in the conventional support, calcined SBA-15, which does not contain a template. The Cu and Zn precursors were introduced to the confined space in the AS and were converted to CuO and ZnO during calcination, during which the template was also removed. The results show that up to 5 mmol·g–1 of CuO and ZnO can be well dispersed; however, severe aggregation of both oxides takes place in the sample derived from the calcined SBA-15 with the same loading. Confined space in the AS and the strong interactions caused by the abundant hydroxyl groups are responsible for the dispersion of CuO and ZnO. The bimetallic materials were employed for the adsorptive separation of propene and propane. The samples prepared from the as-prepared SBA-15 showed superior performance to their counterparts from the calcined SBA-15 in terms of both adsorption capacity of propene and selectivity for propene/propane.

关键词： bimetallic adsorbents     confined space     mesoporous silica     propene/propane separation    

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Development of deep neural network model to predict the compressive strength of FRCM confined columns

Khuong LE-NGUYEN; Quyen Cao MINH; Afaq AHMAD; Lanh Si HO

《结构与土木工程前沿（英文）》 2022年 第16卷 第10期   页码 1213-1232 doi: 10.1007/s11709-022-0880-7

摘要： The present study describes a reliability analysis of the strength model for predicting concrete columns confinement influence with Fabric-Reinforced Cementitious Matrix (FRCM). through both physical models and Deep Neural Network model (artificial neural network (ANN) with double and triple hidden layers). The database of 330 samples collected for the training model contains many important parameters, i.e., section type (circle or square), corner radius rc, unconfined concrete strength fco, thickness nt, the elastic modulus of fiber Ef , the elastic modulus of mortar Em. The results revealed that the proposed ANN models well predicted the compressive strength of FRCM with high prediction accuracy. The ANN model with double hidden layers (APDL-1) was shown to be the best to predict the compressive strength of FRCM confined columns compared with the ACI design code and five physical models. Furthermore, the results also reveal that the unconfined compressive strength of concrete, type of fiber mesh for FRCM, type of section, and the corner radius ratio, are the most significant input variables in the efficiency of FRCM confinement prediction. The performance of the proposed ANN models (including double and triple hidden layers) had high precision with R higher than 0.93 and RMSE smaller than 0.13, as compared with other models from the literature available.

关键词： FRCM     deep neural networks     confinement effect     strength model     confined concrete    

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Fabrication of N-doped carbon nanobelts from a polypyrrole tube by confined pyrolysis for supercapacitors

Wei Wang, Haijun Lv, Juan Du, Aibing Chen

《化学科学与工程前沿（英文）》 2021年 第15卷 第5期   页码 1312-1321 doi: 10.1007/s11705-020-2033-7

摘要： In this present work, N-doped carbon nanobelts (N-CNBs) were prepared by a confined-pyrolysis approach and the N-CNBs were derived from a polypyrrole (Ppy) tube coated with a compact silica layer. The silica layer provided a confined space for the Ppy pyrolysis, thereby hindering the rapid overflow of pyrolysis gas, which is the activator for the formation of carbonaceous materials. At the same time, the confined environment can activate the carbon shell to create a thin wall and strip the carbon tube into belt morphology. This process of confined pyrolysis realizes self-activation during the pyrolysis of Ppy to obtain the carbon nanobelts without adding any additional activator, which reduces pollution and preparation cost. In addition, this approach is simple to operate and avoids the disadvantages of other methods that consume time and materials. The as-prepared N-CNB shows cross-linked nanobelt morphology and a rich porous structure with a large specific surface area. As supercapacitor electrode materials, the N-CNB can present abundant active sites, and exhibits a specific capacitance of 246 F·g , and excellent ability with 95.44% retention after 10000 cycles. This indicates that the N-CNB is an ideal candidate as a supercapacitor electrode material.

关键词： carbon nanobelts     polypyrrole     N-doped     confined pyrolysis     supercapacitor    

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Ductility improvement of GFRP-RC beams using precast confined concrete block in compression zone

《结构与土木工程前沿（英文）》 doi: 10.1007/s11709-023-0968-8

摘要： Fiber-reinforced polymers (FRPs) have received considerable research attention because of their high strength, corrosion resistance, and low weight. However, owing to the lack of ductility in this material and the quasi-brittle behavior of concrete, FRP-reinforced concrete (FRP-RC) beams, even with flexural failure, do not fail in a ductile manner. Because the limited deformation capacity of FRP-RC beams depends on the ductility of their compression zones, the present study proposes using a precast confined concrete block (PCCB) in the compression zone to improve the ductility of the beams. A control beam and four beams with different PCCBs were cast and tested under four-point bending conditions. The control beam failed due to shear, and the PCCBs exhibited different confinements and perforations. The goal was to find an appropriate PCCB for use in the compression zone of the beams, which not only improved the ductility but also changed the failure mode of the beams from shear to flexural. Among the employed blocks, a ductile PCCB with low equivalent compressive strength increased the ductility ratio of the beam to twice that of the control beam. The beam failed in pure flexure with considerable deformation capacity and without significant stiffness reduction.

关键词： ductility     four-point bending test     glass fiber-reinforced polymer     precast confined concrete block    

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Centrifuge model test and field measurement analysis for foundation pit with confined water

Chunlin DING , Xiaohong MENG ,

《结构与土木工程前沿（英文）》 2009年 第3卷 第3期   页码 299-304 doi: 10.1007/s11709-009-0035-0

摘要： The similarity law of centrifuge test was developed for the seepage field and stress field of a foundation pit with confined water by analyzing control equations, and a similarity index and a similarity coefficient of centrifuge test were obtained. Based on the deep foundation pit of the Huangxing Road Station of the Shanghai metro line M8, the deformation stability of the pit was tested. Finally, a comparative study was conducted on the test results of the pit deformation and the field measurement results. Comparison results show that the pit deformation regularity of the test is basically identical with that of the field measurement, and the difference in pit deformation between the test and the field measurement is within 50%. The centrifuge model test can effectively simulate the displacement response of the ground and retaining structure during dewatering and excavation for the pit with confined water, which provides a reliable basis for the design and construction of the pit with confined water.

关键词： foundation pit with confined water     centrifuge model test     seepage-stress coupling field     similarity relation     field measurement     deformation    

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Confined masonry as practical seismic construction alternative–the experience from the 2014 Cephalonia

Fillitsa KARANTONI, Stavroula PANTAZOPOULOU, Athanasios GANAS

《结构与土木工程前沿（英文）》 2018年 第12卷 第3期   页码 270-290 doi: 10.1007/s11709-017-0390-1

摘要：

During August 1953 three strong earthquakes of magnitude ranging from 6.3 to 7.2 shook the Ionian Island of Cephalonia (Kefalonia), Greece, and destroyed almost the entire building stock of the Island which consisted primarily of traditional unreinforced masonry (URM) houses. The authorities went on to restructuring of the building stock, using a structural system that is most like what is known today as confined masonry. They designed about 14 types of one- to two-storey buildings providing the engineers with detailed construction plans. These buildings are known as “Arogi” buildings (Arogi in Greek meaning Aid). On the 24th of January and 3rd of February 2014, two earthquakes of magnitude 6.1 and 6.0 struck the island, causing significant soil damages, developing excessively high ground accelerations. Surprisingly, no damage was reported in the “Arogi” buildings. The seismic behavior of the buildings is examined by FEM linear analysis and it is compared to that of URM structures. Computed results illustrate that the displacements of identical URM buildings would be about twice the magnitudes observed in the corresponding “Arogi” ones, with the implication that the earthquake sequence of 2014 would have caused critical damage should the type of structure be of the URM type. Furthermore, it is illustrated that this low cost alternative method of construction is a very effective means of producing earthquake resilient structures, whereas further reduction of seismic displacement may be achieved in the order of 50% with commensurate effects on damage potential, when reinforced slabs are used to replace the timber roofs.

关键词： Cephalonia     confined masonry     comparative FEM analysis     unreinforced masonry     seismic damage    

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Nano-confined ammonia borane for chemical hydrogen storage

M. A. WAHAB, Huijun ZHAO, X. D. YAO

《化学科学与工程前沿（英文）》 2012年 第6卷 第1期   页码 27-33 doi: 10.1007/s11705-011-1171-3

摘要： There is a great demand for a sufficient and sustainable energy supply. Hence, the search for applicable hydrogen storage materials is extremely important owing to the diversified merits of hydrogen energy. In this regard, ammonia borane (NH BH , AB) containing 19.6 wt-% hydrogen has been considered as a promising material for hydrogen storage applications to realize the “hydrogen economy”, but with limits from slow kinetics of hydrogen release and by-product of trace gases such as ammonia and borazine. In this review, we introduce the recent research on AB, regarding to the nanoconfinement effect on improving the kinetics at a relatively low temperature and the prevention/reduction of undesirable gas formation.

关键词： ammonia borane     hydrogen storage    

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Morphologies of diblock copolymer confined in a slit with patterned surfaces studied by dissipative particle

FENG Jian, HUANG Yongmin, LIU Honglai, HU Ying

《化学科学与工程前沿（英文）》 2007年 第1卷 第2期   页码 132-139 doi: 10.1007/s11705-007-0025-5

摘要： Diblock copolymers with ordered mesophase structures have been used as templates for nano-fabrication. Unfortunately, the ordered structure only exists at micrometer-scale areas, which precludes its use in many advanced applications. To overcome this disadvantage, the diblock copolymer confined in a restricted system with a patterned surface is proved to be an effective means to prohibit the formation of defects and obtain perfect ordered domains. In this work, the morphologies of a thin film of diblock copolymer confined between patterned and neutral surfaces were studied by dissipative particle dynamics. It is shown that the morphology of the symmetric diblock copolymer is affected by the ratio of the pattern period on the surface to the lamellar period of the symmetric diblock copolymer and by the repulsion parameters between blocks and wall particles. To eliminate the defects in the lamellar phase, the pattern period on the surface must match the lamellar period. The difference in the interface energy of different compartments of the pattern should increase with increasing film thickness. The pattern period on the surface has a scaling relationship with the chain length, which is the same as that between the lamellar period and the chain length. The lamellar period is also affected by the polydispersity of the symmetric diblock copolymer. The total period is the average of the period of each component multiplied by the weight of its volume ratio. The morphologies of asymmetric diblock copolymers are also affected by the pattern on the surface, especially when the matching period of the asymmetric diblock copolymer is equal to the pattern period, which is approximately equal to the lamellar period of a symmetric diblock copolymer with the same chain length.

关键词： weight     nano-fabrication     morphology     matching     dissipative particle    

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Interlayer-confined two-dimensional manganese oxide-carbon nanotube catalytic ozonation membrane for

《化学科学与工程前沿（英文）》 2022年 第16卷 第5期   页码 731-744 doi: 10.1007/s11705-021-2110-6

摘要： Catalytic ozonation technology has attracted copious attention in water purification owing to its favorable oxidative degradation of pollutants and mitigation of membrane fouling capacity. However, its extensive industrial application has been restricted by the low ozone utilization and limited mass transfer of the short-lived radical species. Interlayer space-confined catalysis has been theoretically proven to be a viable strategy for achieving high catalytic efficiency. Here, a two-dimensional MnO2-incorporated ceramic membrane with tunable interspacing, which was obtained via the intercalation of a carbon nanotube, was designed as a catalytic ozonation membrane reactor for degrading methylene blue. Benefiting from the abundant catalytic active sites on the surface of two-dimensional MnO2 as well as the ultralow mass transfer resistance of fluids due to the nanolayer confinement, an excellent mineralization effect, i.e., 1.2 mg O3(aq) mg–1 TOC removal (a total organic carbon removal rate of 71.5%), was achieved within a hydraulic retention time of 0.045 s of pollutant degradation. Further, the effects of hydraulic retention time and interlayer spacing on methylene blue removal were investigated. Moreover, the mechanism of the catalytic ozonation employing catalytic ozonation membrane was proposed based on the contribution of the Mn(III/IV) redox pair to electron transfer to generate the reactive oxygen species. This innovative two-dimensional confinement catalytic ozonation membrane could act as a nanoreactor and separator to efficiently oxidize organic pollutants and enhance the control of membrane fouling during water purification.

关键词： catalytic membrane reactor     catalytic ozonation     nanoconfinement     two-dimensional manganese oxide    

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Axial compression behavior of CFRP-confined rectangular concrete-filled stainless steel tube stub column

《结构与土木工程前沿（英文）》 2021年 第15卷 第5期   页码 1144-1159 doi: 10.1007/s11709-021-0762-4

摘要： The mechanical properties of CFRP-confined rectangular concrete-filled stainless steel tube (CFSST) stub columns under axial compression were experimentally studied. A total of 28 specimens (7 groups) were fabricated for the axial compression test to study the influences of length-to-width ratio, CFRP constraint coefficient, and the thickness of stainless steel tube on the axial compression behavior. The specimen failure modes, the stress development of stainless steel tube and CFRP wrap, and the load–strain ratio curves in the loading process were obtained. Meanwhile, the relationship between axial and transverse deformations of each specimen was analyzed through the typical relative load−strain ratio curves. A bearing capacity prediction method was proposed based on the twin-shear strength theory, combining the limit equilibrium state of the CFRP-confined CFSST stub column under axial compression. The prediction method was calibrated by the test data in this study and other literature. The results show that the prediction method is of high accuracy.

关键词： CFRP     rectangular CFSST stub column     bearing capacity     limit equilibrium state     twin-shear strength theory    

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Axial compression tests and numerical simulation of steel reinforced recycled concrete short columns confined

Hui MA; Fangda LIU; Yanan WU; Xin A; Yanli ZHAO

《结构与土木工程前沿（英文）》 2022年 第16卷 第7期   页码 817-842 doi: 10.1007/s11709-022-0844-y

摘要： To research the axial compression behavior of steel reinforced recycled concrete (SRRC) short columns confined by carbon fiber reinforced plastics (CFRP) strips, nine scaled specimens of SRRC short columns were fabricated and tested under axial compression loading. Subsequently, the failure process and failure modes were observed, and load-displacement curves as well as the strain of various materials were analyzed. The effects on the substitution percentage of recycled coarse aggregate (RCA), width of CFRP strips, spacing of CFRP strips and strength of recycled aggregate concrete (RAC) on the axial compression properties of columns were also analyzed in the experimental investigation. Furthermore, the finite element model of columns which can consider the adverse influence of RCA and the constraint effect of CFRP strips was founded by ABAQUS software and the nonlinear parameter analysis of columns was also implemented in this study. The results show that the first to reach the yield state was the profile steel in the columns, then the longitudinal rebars and stirrups yielded successively, and finally RAC was crushed as well as the CFRP strips was also broken. The replacement rate of RCA has little effect on the columns, and with the substitution rate of RCA from 0 to 100%, the bearing capacity of columns decreased by only 4.8%. Increasing the CFRP strips width or decreasing the CFRP strips spacing could enhance the axial bearing capacity of columns, the maximum increase was 10.5% or 11.4%, and the ductility of columns was significantly enhanced. Obviously, CFRP strips are conducive to enhance the axial bearing capacity and deformation capacity of columns. On this basis, considering the restraint effect of CFRP strips and the adverse effects of RCA, the revised formulas for calculating the axial bearing capacity of SRRC short columns confined by CFRP strips were proposed.

关键词： steel reinforced recycled concrete     CFRP strips     short columns     axial compression behavior     recycled aggregate concrete    

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Ultrafine Fe-modulated Ni nanoparticles embedded within nitrogen-doped carbon from Zr-MOFs-confined conversion

《化学科学与工程前沿（英文）》 2022年 第16卷 第7期   页码 1114-1124 doi: 10.1007/s11705-021-2087-1

摘要： Improvement of the low-cost transition metal electrocatalyst used in sluggish oxygen evolution reaction is a significant but challenging problem. In this study, ultrafine Fe-modulated Ni nanoparticles embedded in a porous Ni-doped carbon matrix were produced by the pyrolysis of zirconium metal-organic-frameworks, in which 2,2′-bipyridine-5,5′-dicarboxylate operating as a ligand can coordinate with Ni2+ and Fe3+. This strategy allows formation of Fe-modulated Ni nanoparticles with a uniform dimension of about 2 nm which can be ascribed to the spatial blocking effect of ZrO2. This unique catalyst displays an efficient oxygen evolution reaction electrocatalytic activity with a low overpotential of 372 mV at 10 mA·cm–2 and a small Tafel slope of 84.4 mV·dec–1 in alkaline media. More importantly, it shows superior durability and structural stability after 43 h in a chronoamperometry test. Meanwhile, it shows excellent cycling stability during 4000 cyclic voltammetry cycles. This research offers a new insight into the construction of uniform nanoscale transition metals and their alloys as highly efficient and durable electrocatalysts.

关键词： metal-organic framework     pyrolysis     ultrafine     Fe-modulated Ni nanoparticles     oxygen evolution reaction    

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The “Tiangong” Chinese Space Station project

Yang HONG

《工程管理前沿（英文）》 2018年 第5卷 第2期   页码 278-283 doi: 10.15302/J-FEM-2018202

关键词： manned space station     space station project     basic design    

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Application and development of modern long-span space structures in China

Shilin DONG, Yang ZHAO, Dong XING

《结构与土木工程前沿（英文）》 2012年 第6卷 第3期   页码 224-239 doi: 10.1007/s11709-012-0166-6

摘要： Modern long-span space structures, developed during the 1970s and 1980s, are light and effective structures based on new technologies and light-weight high-strength materials, such as membranes and steel cables. These structures include air-supported membrane structures, cable-membrane structures, cable truss structures, beam string structures, suspen-domes, cable domes, composite structures of cable dome and single-layer lattice shell, Tensairity structures and so forth. For the premodern space structures widely used since the mid-twentieth century (such as thin shells, space trusses, lattice shells and ordinary cable structures), new space structures have been developed by the combination of different structural forms and materials. The application of prestressing technology and the innovation of structural concepts and configurations are also associated with modern space structures, including composite space trusses, open-web grid structures, polyhedron space frame structures, partial double-layer lattice shells, cable-stayed grid structures, tree-type structures, prestressed segmental steel structures and so forth. This paper provides a review of the structural characteristics and practical applications in China of modern rigid space structures, modern flexible space structures and modern rigid-flexible combined space structures.

关键词： modern long-span space structures     rigid space structures     flexible space structures     rigid-flexible combined space structures     application and development    

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统筹空间科学、空间技术、空间应用协调发展的思考

周建平,吴季

《中国工程科学》 2023年 第25卷 第2期   页码 59-66 doi: 10.15302/J-SSCAE-2023.02.007

摘要：

我国航天事业因历史原因和投入限制，在初期以空间技术、空间应用为主，对空间科学重视不足，空间科学、空间技术、空间应用基本上是独立发展的；着眼新时期航天强国建设，需要将空间技术的发展深度融合到空间科学、空间应用中去，从而创造新的机遇和成就。本文剖析了空间科学、空间技术、空间应用的基本内涵并明确三者的相互关系，在系统分析国际空间科学、空间技术、空间应用的整体态势，细致梳理我国相关领域发展情况的基础上，论证了统筹我国空间科学、空间技术、空间应用协调发展的必要性，凝练了三者协调发展面临的主要问题。空间科学、空间技术、空间应用之间既有需求交叉，又可互促带动，应在规划、部署、实施的全过程中进行统筹考虑：发挥新型举国体制优势，在统一管理下做好顶层规划；坚持创新驱动发展战略，以技术进步抢占国际航天制高点；支持空间领域基础研究，培育高水平的科学家和工程师队伍；加强资源统筹协调，促进空间应用数据的合理开放和充分利用。

关键词： 航天事业；空间科学；空间技术；空间应用；协调发展；数据开放共享    

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标题 作者 时间 类型 操作

Fabrication of bimetallic Cu–Zn adsorbents with high dispersion by using confined space for gas adsorptive

期刊论文

Development of deep neural network model to predict the compressive strength of FRCM confined columns

Khuong LE-NGUYEN; Quyen Cao MINH; Afaq AHMAD; Lanh Si HO

期刊论文

Fabrication of N-doped carbon nanobelts from a polypyrrole tube by confined pyrolysis for supercapacitors

Wei Wang, Haijun Lv, Juan Du, Aibing Chen

期刊论文

Ductility improvement of GFRP-RC beams using precast confined concrete block in compression zone

期刊论文

Centrifuge model test and field measurement analysis for foundation pit with confined water

Chunlin DING , Xiaohong MENG ,

期刊论文

Confined masonry as practical seismic construction alternative–the experience from the 2014 Cephalonia

Fillitsa KARANTONI, Stavroula PANTAZOPOULOU, Athanasios GANAS

期刊论文

Nano-confined ammonia borane for chemical hydrogen storage

M. A. WAHAB, Huijun ZHAO, X. D. YAO

期刊论文

Morphologies of diblock copolymer confined in a slit with patterned surfaces studied by dissipative particle

FENG Jian, HUANG Yongmin, LIU Honglai, HU Ying

期刊论文

Interlayer-confined two-dimensional manganese oxide-carbon nanotube catalytic ozonation membrane for

期刊论文

Axial compression behavior of CFRP-confined rectangular concrete-filled stainless steel tube stub column

期刊论文

Axial compression tests and numerical simulation of steel reinforced recycled concrete short columns confined

Hui MA; Fangda LIU; Yanan WU; Xin A; Yanli ZHAO

期刊论文

Ultrafine Fe-modulated Ni nanoparticles embedded within nitrogen-doped carbon from Zr-MOFs-confined conversion

期刊论文

The “Tiangong” Chinese Space Station project

Yang HONG

期刊论文

Application and development of modern long-span space structures in China

Shilin DONG, Yang ZHAO, Dong XING

期刊论文

统筹空间科学、空间技术、空间应用协调发展的思考

周建平,吴季

期刊论文